Laboratory for Light Elements Study

Laboratory for Light Elements Study

Within the Laboratory for Light Elements Studies (LEEL), research themes focus on the behavior of light elements in materials for energy. Activities range from material synthesis to characterizations, which include those obtained with the laboratory’s specific tool, the nuclear microprobe, an instrument particularly suited to monitoring light elements.

Our objective is to acquire fundamental knowledge regarding emerging materials used, or envisioned, for low carbon fingerprint energy sources, such as post Li-ion electrochemical accumulators and nuclear materials.

Within the LEEL, we have access to various physical chemical synthesis methods, from solution chemistry to innovative gas pathway, virtually allowing synthesis of any material with controlled stoichiometry and size.

We synthesize new materials for high performance electrodes or solid-state electrolytes for post Li-ion batteries. We also explore innovative liquid electrolytes such as water in slat type, and conduct various electrochemical investigations on assemblies together with accelerated aging studies using radiolysis (in collaboration with LIONS laboratory).

The nuclear microprobe facility, hosted in LEEL laboratory, is principally used for our research topics. It is based on the spectroscopy of emitted species (photons, particles) following the interaction of an energetic light ion beam with the studied samples. Processes of diffusion and transport, precipitation and segregation of light elements can be understood locally using judiciously chosen nuclear reactions, whether by using isotopic tracers or by directly measuring the desired element. Therefore, we can chemically characterize as prepared materials or assemblies, and also extend studies by developing setups for operando monitoring.

The nuclear microprobe facility also offers a unique feature since it is equipped with a hot beamline devoted to radioactive samples. We therefore provide analytical expertise for materials like highly irradiating nuclear fuel claddings.

As part of EMIR&A research infrastructure, we also provide expertise and contribute to scientific collaborations for various research fields and groups requiring nuclear microprobe experiments.

Projets

  • ANR-MAGWAT

    Innovative energy storage based on magnesium and aqueous electrolytes Aqueous solutions play a key role in biology, chemistry and, more particularly, in energy-related fields such as photo and electro-catalysis and batteries. Whereas aqueous batteries are supposed to be constrained by the thermodynamic electrochemical stability window of water (1.23 V vs. NHE under standard conditions in…

  • Exploratory PEPR DIADEM- FASTNANO

    Exploratory PEPR DIADEM- FASTNANO

    IRAMIS/NIMBE is coordinating one of the projects, FastNano, which aims to target and strengthen research into 0, 1 and 2D nano-objects that can be used for innovative applications in the fields of renewable energies (materials for all-solid-state batteries, electro- and photo-catalysis, photovoltaics…), healthcare (biological marking, nanomedicine, diagnostics…) and electronics (MIM- Metal-Isolant-Metal diodes, optoelectronics…) The aim…

  • Iramis partner of the European RISEnergy project

    Iramis partner of the European RISEnergy project

    Le CEA-Iramis est partenaire du projet Européen Infrastructures “RISEnergy” qui rassemble un ensembled’entreprises, d’organismes de recherche, d’Universités et d’agences de financement européens (69…

  • PEPR-OPENSTORM

    PEPR-OPENSTORM

    Operando characterization of materials for energy storage: from the laboratory to large-scale instruments The OPENSTORM project has set itself the challenge of establishing a French characterization platform with the tools, methods and organizational flows needed to provide rapid answers, over the coming years, to the scientific questions critical to the viability of the batteries of…

Thèses

Thèmes de recherche

  • Advanced Synthesis

    LEEL’s FSP burner operating for Al2O3 nanoparticles synthesis : left pilot flame, middle pure ethanol spray, right synthesis flame with Al nitrate/ethanol spray.

  • Characterization of materials for energy

    Characterization of materials for energy

    Les différentes filières énergétiques, telles que l’énergie nucléaire ou encore les nouvelles technologies autour de l’hydrogène, vecteur énergétique, ou le photovoltaïque, demandent des matériaux…

  • Ion Beam Analysis

    Ion Beam Analysis

    The nuclear microprobe is a non-destructive analysis tool allowing elemental characterization at the micrometer scale of solid samples of diverse origins: interfaces and grains of synthesized materials, cellular monolayers, inclusions in terrestrial and extraterrestrial geologic samples. The method relies on the detection and spectrometry of emitted radiations by the interaction of a light ion micro-beam…

  • Post Li-Ion Batteries

    Liquid Electrolyte based Multivalent Batteries The development of lithium-ion batteries has played a key role in this development of intermittent renewable energies and mobile technologies. However, this technology seems to be reaching its limits and new solutions are emerging, such as magnesium batteries. Magnesium metal is an attractive negative electrode because of its abundance and…

  • Post Li-ion Batteries

    Post Li-ion Batteries

    The battery research group at LEEL investigates physicochemical and mechanistic processes occurring at the interface and in the bulk of post-Li-ion batteries to create a fundamental understanding. Our research mainly focuses on developing a fundamental understanding of the various processes taking place in the electrode and electrolyte by developing various in-situ/operando characterization techniques. The aim…